Aim: To demonstrate the principles of colorimerty and the use of known standard solutions in QUANTITATIVE ANALYSIS by electronic equipment.
Procedure:
1. 39.34g of CuSO4.5H2O was dissolved in distilled water and made up to 500.0cm^3. This was used as a stock soultion for the standards constructed for this exercise. If Mr(CuSO4.5H2O) is 249.96 and Mr(cu)= 63.54, find the mass of Cu in the stock solution in grams per liter (g/L) and in parts per million (ppm). (Assume the density of the solution is 1.00g/cm^3)
2. The "known standards" used to construct the calibration curve were made up according the following table. Use the stock solution concentration and appropriate dilution factors to calculate the concentration of each of the standards prepared.
The standards are in blue color so we analyze with a light color which is absorbed the most. what should we use? (We have a limited choice in this case).
3. Starting with the weakest standard, put about 20ml in a clean cell and find the adsorbance reading using the appropriate light source. Rinse the cell and test all the standards.
4. Plot a neat graph of ABSORBANCE Vs CONCENTRATION
5. Run samples of UNKNOWNs through the colorimeter and record the results. Use the graph to determine the concentration of copper ions in each of them.
Okay, thats a practice PRAC SAC, and my own PRAC SAC is prob very close to this one, maybe with just a different substance or something lets hope ><
Umm, im missing the table, but ill scan that later, and yeah i realise i could of scaned the whole sheet but i was nearly done anyways so yeah =="
FIRST THING; i want to ask.. the weight of Cu is 10.00g ? 0.0 Yes/No? Probably no LOL